Dynamic compression induced solidification

Roth B, Wildner W, Drummer D (2020)

Publication Type: Journal article

Publication year: 2020


Book Volume: 12

Article Number: 488

Journal Issue: 2

DOI: 10.3390/polym12020488


This study presents a method for the determination of the dynamic pressure-dependent solidification of polycarbonate (PC) during flow using high pressure capillary rheometer (HPC) measurements. In addition, the pressure-dependent solidification was determined by isothermal pressure-volume-temperature (pvT)measurements under static conditionswithout shear. Independent of the compression velocity, a linear increase of the solidification pressure with temperature could be determined. Furthermore, the results indicate that the relaxation time at a constant temperature and compression rate can increase to such an extent that the material can no longer follow within the time scale specified by the compression rate. Consequently, the flow through the capillary stops at a specific pressure, with higher compression rates resulting in lower solidification pressures. Consequently, in regard to HPC measurements, it could be shown that the evaluation of the pressure via a pressure hole can lead to measurement errors in the limit range. Since the filling process in injection molding usually takes place under such transient conditions, the results are likely to be relevant for modelling the flow processes of thin-walled and microstructures with high aspect ratios.

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Roth, B., Wildner, W., & Drummer, D. (2020). Dynamic compression induced solidification. Polymers, 12(2). https://doi.org/10.3390/polym12020488


Roth, Benedikt, Wolfgang Wildner, and Dietmar Drummer. "Dynamic compression induced solidification." Polymers 12.2 (2020).

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