Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides

Schimmel S, Künecke U, Baser HH, Steigerwald T, Hertweck B, Alt N, Schlücker E, Schwieger W, Wellmann P (2014)

Publication Language: English

Publication Status: Published

Publication Type: Journal article

Publication year: 2014

Journal

Physica Status Solidi (C) Current Topics in Solid State Physics Wiley - V C H Verlag GmbbH & Co.

Publisher: Wiley - V C H Verlag GmbbH & Co.

Book Volume: 11

Pages Range: 1439-1442

DOI: 10.1002/pssc.201300656

Abstract

In-situ X-ray visualization of hydrothermal growth of silicalite- 1 is applied as an intermediate step for developing X-ray in-situ visualization techniques for ammonothermal growth of nitride materials. In-situ X-ray imaging of silicalite-1 crystals grown by the bulk material dissolution technique (Shimizu and Hamada, Angew. Chem., Int. Ed. 38, 2725 (1999) [1]) is demonstrated using a stainless steel autoclave equipped with ceramic aluminium oxide windows. Processes in the reaction medium such as local density changes are also visualized. The transferability of the technique to ammonothermal growth of nitrides is evaluated. Furthermore, the applicability of windowless autoclaves for X-ray in-situ monitoring of ammonothermal crystal growth of nitrides is investigated. (C) 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

Authors with CRIS profile

Saskia Schimmel Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik) Ulrike Künecke Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik) Hasan-Hüseyin Baser Professur für Technische Chemie (Reaktionstechnik) Thomas Steigerwald Lehrstuhl für Prozessmaschinen und Anlagentechnik Benjamin Hertweck Lehrstuhl für Prozessmaschinen und Anlagentechnik Nicolas Alt Lehrstuhl für Prozessmaschinen und Anlagentechnik Eberhard Schlücker Lehrstuhl für Prozessmaschinen und Anlagentechnik Wilhelm Schwieger Professur für Technische Chemie (Reaktionstechnik) Peter Wellmann Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik)

How to cite

APA:

Schimmel, S., Künecke, U., Baser, H.-H., Steigerwald, T., Hertweck, B., Alt, N.,... Wellmann, P. (2014). Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides. Physica Status Solidi (C) Current Topics in Solid State Physics, 11, 1439-1442. https://doi.org/10.1002/pssc.201300656

MLA:

Schimmel, Saskia, et al. "Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides." Physica Status Solidi (C) Current Topics in Solid State Physics 11 (2014): 1439-1442.

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