Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange

Krauss SW, Schweins R, Magerl A, Zobel M (2019)

Publication Type: Journal article

Publication year: 2019

Journal

Journal of Applied Crystallography International Union of Crystallography

Book Volume: 52

Pages Range: 284-288

DOI: 10.1107/S1600576719000906

Abstract

The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering.

Authors with CRIS profile

Andreas Magerl Lehrstuhl für Biophysik

Involved external institutions

Universität Bayreuth DE Germany (DE) Institute Laue-Langevin (ILL) FR France (FR)

How to cite

APA:

Krauss, S.W., Schweins, R., Magerl, A., & Zobel, M. (2019). Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange. Journal of Applied Crystallography, 52, 284-288. https://dx.doi.org/10.1107/S1600576719000906

MLA:

Krauss, Sebastian W., et al. "Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange." Journal of Applied Crystallography 52 (2019): 284-288.

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