Journal article
(Original article)


The stopped-drop method: A novel setup for containment-free and time-resolved measurements


Publication Details
Author(s): Schiener A, Seifert S, Magerl A
Publisher: International Union of Crystallography
Publication year: 2016
Volume: 23
Journal issue: 2
Pages range: 545-550
ISSN: 1600-5775
Language: English

Abstract

A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the volution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.



How to cite
APA: Schiener, A., Seifert, S., & Magerl, A. (2016). The stopped-drop method: A novel setup for containment-free and time-resolved measurements. Journal of Synchrotron Radiation, 23(2), 545-550. https://dx.doi.org/10.1107/S1600577515023826

MLA: Schiener, Andreas, Soenke Seifert, and Andreas Magerl. "The stopped-drop method: A novel setup for containment-free and time-resolved measurements." Journal of Synchrotron Radiation 23.2 (2016): 545-550.

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