Journal article


Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides


Publication Details
Author(s): Schimmel S, Künecke U, Baser HH, Steigerwald T, Hertweck B, Alt N, Schlücker E, Schwieger W, Wellmann P
Publisher: Wiley - V C H Verlag GmbbH & Co.
Publication year: 2014
Volume: 11
Pages range: 1439-1442
ISSN: 1862-6351
eISSN: 1610-1642
Language: English

Abstract

In-situ X-ray visualization of hydrothermal growth of silicalite- 1 is applied as an intermediate step for developing X-ray in-situ visualization techniques for ammonothermal growth of nitride materials. In-situ X-ray imaging of silicalite-1 crystals grown by the bulk material dissolution technique (Shimizu and Hamada, Angew. Chem., Int. Ed. 38, 2725 (1999) [1]) is demonstrated using a stainless steel autoclave equipped with ceramic aluminium oxide windows. Processes in the reaction medium such as local density changes are also visualized. The transferability of the technique to ammonothermal growth of nitrides is evaluated. Furthermore, the applicability of windowless autoclaves for X-ray in-situ monitoring of ammonothermal crystal growth of nitrides is investigated. (C) 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim



Focus Area of Individual Faculties


How to cite
APA: Schimmel, S., Künecke, U., Baser, H.-H., Steigerwald, T., Hertweck, B., Alt, N.,... Wellmann, P. (2014). Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides. Physica Status Solidi (C) Current Topics in Solid State Physics, 11, 1439-1442. https://dx.doi.org/10.1002/pssc.201300656

MLA: Schimmel, Saskia, et al. "Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides." Physica Status Solidi (C) Current Topics in Solid State Physics 11 (2014): 1439-1442.

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