Influence of magnesium doping on the phase transformation temperature of Beta-TCP ceramics examined by Rietveld refinement
Enderle R, Götz-Neunhoeffer F, Göbbels M, Müller F, Greil P (2005)
Publication Language: English
Publication Type: Journal article
Publication year: 2005
Journal
Publisher: Elsevier
Book Volume: Vol. 26
Pages Range: 3379-3384
Journal Issue: 17
DOI: 10.1016/j.biomaterials.2004.09.017
Abstract
The influence of Mg doping in Ca 3(PO 4) 2 on the transformation temperature of β-tricalcium phosphate (β-TCP) to α-tricalcium phosphate (α-TCP) was examined. A maximum substitution by 14 mol% of Mg 2+ on Ca 2+ sites in the β-TCP structure was determined for powders calcinated at 1025±10°C. X-ray powder diffraction analysis (XRPD) in combination with Rietveld method (TOPAS 2.1) was employed for quantitative phase analysis and structural refinement. The synthesized and characterized Mg-doped samples were sintered in air atmosphere in a vertical tube furnace at suitable temperatures ranging from 1460 to 1680°C and subsequently quenched to room temperature, in order to stabilize α-TCP. The β to α transformation temperatures were determined by differential temperature analysis and XRPD analysis. © 2004 Elsevier Ltd. All rights reserved.
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APA:
Enderle, R., Götz-Neunhoeffer, F., Göbbels, M., Müller, F., & Greil, P. (2005). Influence of magnesium doping on the phase transformation temperature of Beta-TCP ceramics examined by Rietveld refinement. Biomaterials, Vol. 26(17), 3379-3384. https://dx.doi.org/10.1016/j.biomaterials.2004.09.017
MLA:
Enderle, Ralph, et al. "Influence of magnesium doping on the phase transformation temperature of Beta-TCP ceramics examined by Rietveld refinement." Biomaterials Vol. 26.17 (2005): 3379-3384.
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