Impact of formulation and operating parameters on particle size and grinding media wear in wet media milling of organic compounds – A case study for pyrene
Flach F, Konnerth CG, Peppersack C, Schmidt J, Damm C, Breitung-Faes S, Peukert W, Kwade A (2016)
Publication Language: English
Publication Status: Published
Publication Type: Journal article, Original article
Publication year: 2016
Journal
Publisher: Elsevier B.V.
Book Volume: 27
Pages Range: 2507-2519
Journal Issue: 6
DOI: 10.1016/j.apt.2016.09.026
Abstract
This study presents the influence of process and formulation parameters on fine grinding of the crystalline organic model compound pyrene. Submicron particles were produced by wet media milling in water. By applying an electrosteric stabilization and optimized process parameters, particle sizes below 100 nm were obtained. Additionally, the influence of formulation and process parameters on grinding media wear were investigated. The product formulation with an ionic surfactant and a nonionic polymer was identified as a significant parameter to reduce the grinding wear. Furthermore, the set of operating parameters as well as the choice of grinding media material were found as key parameters to reduce product contamination. Grinding media wear is proportional to the specific energy input and can be minimized by optimizing the stress energy of grinding media.
Authors with CRIS profile
Christoph-Günther Konnerth
Lehrstuhl für Partikelsynthese (LFG)
Jochen Schmidt
Lehrstuhl für Partikelsynthese (LFG)
Cornelia Damm
Lehrstuhl für Partikelsynthese (LFG)
Wolfgang Peukert
Lehrstuhl für Partikelsynthese (LFG)
Involved external institutions
Germany (DE)How to cite
APA:
Flach, F., Konnerth, C.-G., Peppersack, C., Schmidt, J., Damm, C., Breitung-Faes, S.,... Kwade, A. (2016). Impact of formulation and operating parameters on particle size and grinding media wear in wet media milling of organic compounds – A case study for pyrene. Advanced Powder Technology, 27(6), 2507-2519. https://doi.org/10.1016/j.apt.2016.09.026
MLA:
Flach, F., et al. "Impact of formulation and operating parameters on particle size and grinding media wear in wet media milling of organic compounds – A case study for pyrene." Advanced Powder Technology 27.6 (2016): 2507-2519.
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