Investigation of the growth kinetics of SiC crystals during physical vapor transport growth by the application of in-situ 3D computed tomography visualization

Arzig M, Salamon M, Uhlmann N, Wellmann P (2019)


Publication Language: English

Publication Status: Accepted

Publication Type: Journal article

Future Publication Type: Journal article

Publication year: 2019

Journal

Article Number: 1900778

DOI: 10.1002/adem.201900778

Abstract

Computed tomography using X‐rays has been applied during bulk growth of SiC in order to investigate growth kinetics in‐situ during the physical vapor transport process. Besides the standard SiC source material, in particular a pure solid source SiC block is used. It is found that the growth rate is lowered as the sublimation of gaseous species is limited to the top part of the solid source. The morphological changes in the source area during growth differ significantly compared to the process when conventional powder is used. The formation of multiple growth centers on the surface of the seed is monitored in‐situ with a computed tomography system. In a series of experiments the influence of the supersaturation on the growth is examined. The in‐situ computed tomography shows that the curvature of the growth interface is stronger influenced by the thermal field at higher pressures. A high supersaturation leads to the formation of rather smooth surface morphologies while the formation of large steps on the surface was induced at lower supersaturations.

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APA:

Arzig, M., Salamon, M., Uhlmann, N., & Wellmann, P. (2019). Investigation of the growth kinetics of SiC crystals during physical vapor transport growth by the application of in-situ 3D computed tomography visualization. Advanced Engineering Materials. https://dx.doi.org/10.1002/adem.201900778

MLA:

Arzig, Matthias, et al. "Investigation of the growth kinetics of SiC crystals during physical vapor transport growth by the application of in-situ 3D computed tomography visualization." Advanced Engineering Materials (2019).

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