Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties

Machoke A, Knoke IY, Lopez-Orozco S, Schmiele M, Selvam T, Marthala VRR, Spiecker E, Unruh T, Hartmann M, Schwieger W, Hartmann M, Spiecker E (2014)

Publication Status: Published

Publication Type: Journal article, Original article

Publication year: 2014

Journal

Microporous and Mesoporous Materials Elsevier

Publisher: Elsevier

Book Volume: 190

Pages Range: 324-333

DOI: 10.1016/j.micromeso.2014.02.026

Abstract

The formation of multilamellar MFI-type zeolite has been studied systematically by investigating the crystallization kinetics and the influence of different synthesis parameters under static conditions. Depending on the template amount and alkalinity, multilamellar MFI-type zeolites with different degrees of purity were obtained. In accordance with X-ray diffraction, SAXS and SEM results, highly crystalline multilamellar MFI-type zeolites were obtained within 4 days of crystallization time. Depending on the Si/Al ratio of the synthesis gel, different crystallization rates, textural properties and product morphologies were observed. (C) 2014 Elsevier Inc. All rights reserved.

Authors with CRIS profile

Albert Machoke Lehrstuhl für Chemische Reaktionstechnik (CRT) Martin Schmiele Lehrstuhl für Kristallographie und Strukturphysik (ICSP) Tobias Unruh Professur für Nanomaterialcharakterisierung (Streumethoden) Wilhelm Schwieger Professur für Technische Chemie (Reaktionstechnik) Martin Hartmann Professur für Katalyse Erdmann Spiecker Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung)

Additional Organisation(s)

Exzellenz-Cluster Engineering of Advanced Materials (EAM) Interdisziplinäres Zentrum, Center for Nanoanalysis and Electron Microscopy (CENEM)

How to cite

APA:

Machoke, A., Knoke, I.Y., Lopez-Orozco, S., Schmiele, M., Selvam, T., Marthala, V.R.R.,... Spiecker, E. (2014). Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties. Microporous and Mesoporous Materials, 190, 324-333. https://doi.org/10.1016/j.micromeso.2014.02.026

MLA:

Machoke, Albert, et al. "Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties." Microporous and Mesoporous Materials 190 (2014): 324-333.

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