Bauer W, Soi A, Hirsch A (2000)
Publication Type: Journal article, Original article
Publication year: 2000
Original Authors: Bauer W., Soi A., Hirsch A.
Publisher: Wiley-Blackwell
Book Volume: 38
Pages Range: 500-503
Journal Issue: 7
URI: https://www.scopus.com/record/display.uri?eid=2-s2.0-0034214655&origin=inward
In a modification of the well-established DPFGSE-NOE method, the mixing period is replaced by a spin-lock sequence (DPFGSE-ROE). Similar to conventional one- and two-dimensional ROE applications, the NOE is positive throughout, irrespective of the molecular correlation time. For the two calixarene derivatives 1 and 2 conventional difference NOE spectroscopy and DPFGSE-NOE yield negative NOEs, indicating ωτ > 1.12. By contrast, DPFGSE-ROE leads to strong positive enhancements. Indirect (transferred) NOEs may be identified by their negative sign under these conditions. Copyright © 2000 John Wiley & Sons, Ltd.
APA:
Bauer, W., Soi, A., & Hirsch, A. (2000). Application of DPFGSE-ROE to calixarene derivatives under conditions near NOE zero-crossing. Magnetic Resonance in Chemistry, 38(7), 500-503.
MLA:
Bauer, Walter, Antonio Soi, and Andreas Hirsch. "Application of DPFGSE-ROE to calixarene derivatives under conditions near NOE zero-crossing." Magnetic Resonance in Chemistry 38.7 (2000): 500-503.
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