The stopped-drop method: A novel setup for containment-free and time-resolved measurements

Beitrag in einer Fachzeitschrift
(Originalarbeit)


Details zur Publikation

Autor(en): Magerl A, Schiener A, Seifert S
Zeitschrift: Journal of Synchrotron Radiation
Verlag: International Union of Crystallography
Jahr der Veröffentlichung: 2016
Band: 23
Heftnummer: 2
Seitenbereich: 545-550
ISSN: 1600-5775
Sprache: Englisch


Abstract


A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the volution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.



FAU-Autoren / FAU-Herausgeber

Magerl, Andreas Prof. Dr.
Lehrstuhl für Kristallographie und Strukturphysik
Schiener, Andreas
Lehrstuhl für Kristallographie und Strukturphysik


Zusätzliche Organisationseinheit(en)
Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden
Interdisziplinäres Zentrum, Center for Nanoanalysis and Electron Microscopy (CENEM)


Autor(en) der externen Einrichtung(en)
Argonne National Laboratory


Zitierweisen

APA:
Magerl, A., Schiener, A., & Seifert, S. (2016). The stopped-drop method: A novel setup for containment-free and time-resolved measurements. Journal of Synchrotron Radiation, 23(2), 545-550. https://dx.doi.org/10.1107/S1600577515023826

MLA:
Magerl, Andreas, Andreas Schiener, and Soenke Seifert. "The stopped-drop method: A novel setup for containment-free and time-resolved measurements." Journal of Synchrotron Radiation 23.2 (2016): 545-550.

BibTeX: 

Zuletzt aktualisiert 2019-03-06 um 16:33