Schatz J (1998)
Publication Type: Journal article, Original article
Publication year: 1998
Original Authors: Schatz J., Schildbach F., Lentz A., Rastätter S.
Pages Range: 75-77
Journal Issue: 1
URI: https://www.scopus.com/record/display.uri?eid=2-s2.0-0346337238&origin=inward
The solid state inclusion of various organic solvent molecules in p-tert-butylcalix[4]arene and p-tert-butylcalix[6]arene has been studied by thermal gravimetry and electron impact mass spectrometry (EI-MS). The host-guest ratio varies from 1:2 to 4:1 and the nature of included guest has been determined by EI-MS. Thermal gravimetric analysis of solvent-p-tert-butylcalix[n]arene complexes gives a qualitative order of intramolecular forces involved. Structural information obtained by cross-polarization magic angle spinning (CP-MAS) C NMR spectroscopy is in good agreement with known data from single-crystal X-ray diffraction analysis.
APA:
Schatz, J. (1998). Thermal gravimetry, mass spectrometry and solid-state 13C NMR spectroscopy - Simple and efficient methods to characterize the inclusion behaviour of p-tert-butylcalix[n]arenes. Journal of the Chemical Society, Perkin Transactions 2, 1, 75-77.
MLA:
Schatz, Jürgen. "Thermal gravimetry, mass spectrometry and solid-state 13C NMR spectroscopy - Simple and efficient methods to characterize the inclusion behaviour of p-tert-butylcalix[n]arenes." Journal of the Chemical Society, Perkin Transactions 2 1 (1998): 75-77.
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