Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides

Journal article


Publication Details

Author(s): Schimmel S, Künecke U, Baser HH, Steigerwald T, Hertweck B, Alt N, Schlücker E, Schwieger W, Wellmann P
Journal: Physica Status Solidi (C) Current Topics in Solid State Physics
Publisher: Wiley - V C H Verlag GmbbH & Co.
Publication year: 2014
Volume: 11
Pages range: 1439-1442
ISSN: 1862-6351
eISSN: 1610-1642
Language: English


Abstract


In-situ X-ray visualization of hydrothermal growth of silicalite- 1 is applied as an intermediate step for developing X-ray in-situ visualization techniques for ammonothermal growth of nitride materials. In-situ X-ray imaging of silicalite-1 crystals grown by the bulk material dissolution technique (Shimizu and Hamada, Angew. Chem., Int. Ed. 38, 2725 (1999) [1]) is demonstrated using a stainless steel autoclave equipped with ceramic aluminium oxide windows. Processes in the reaction medium such as local density changes are also visualized. The transferability of the technique to ammonothermal growth of nitrides is evaluated. Furthermore, the applicability of windowless autoclaves for X-ray in-situ monitoring of ammonothermal crystal growth of nitrides is investigated. (C) 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim



FAU Authors / FAU Editors

Alt, Nicolas Dr.-Ing.
Lehrstuhl für Prozessmaschinen und Anlagentechnik
Baser, Hasan-Hüseyin Dr.-Ing.
Professur für Technische Chemie (Reaktionstechnik)
Hertweck, Benjamin
Lehrstuhl für Prozessmaschinen und Anlagentechnik
Künecke, Ulrike Dr.-Ing.
Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik)
Schimmel, Saskia
Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik)
Schlücker, Eberhard Prof. Dr.-Ing.
Lehrstuhl für Prozessmaschinen und Anlagentechnik
Schwieger, Wilhelm Prof. Dr.
Professur für Technische Chemie (Reaktionstechnik)
Steigerwald, Thomas
Lehrstuhl für Prozessmaschinen und Anlagentechnik
Wellmann, Peter Prof. Dr.-Ing.
Professur für Werkstoffwissenschaften (Werkstoffe der Elektrotechnik)


How to cite

APA:
Schimmel, S., Künecke, U., Baser, H.-H., Steigerwald, T., Hertweck, B., Alt, N.,... Wellmann, P. (2014). Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides. Physica Status Solidi (C) Current Topics in Solid State Physics, 11, 1439-1442. https://dx.doi.org/10.1002/pssc.201300656

MLA:
Schimmel, Saskia, et al. "Towards X-ray in-situ visualization of ammonothermal crystal growth of nitrides." Physica Status Solidi (C) Current Topics in Solid State Physics 11 (2014): 1439-1442.

BibTeX: 

Last updated on 2018-08-08 at 02:54