Dispersing silicon nanoparticles with a stirred media mill and subsequent functionalization with phenyl acetylene

Reindl A, Cimpean CR, Bauer W, Peukert W, Kryschi C, Comanici R, Ebbers A (2007)


Publication Language: English

Publication Type: Journal article, Original article

Publication year: 2007

Journal

Original Authors: Reindl A., Cimpean C., Bauer W., Comanici R., Ebbers A., Peukert W., Kryschi C.

Publisher: Elsevier

Book Volume: 301

Pages Range: 382-387

DOI: 10.1016/j.colsurfa.2006.12.073

Abstract

Silicon particles were dispersed in 1-butanol using a stirred media mill. Morphology, size and bulk structure of untreated, ground and styrenyl-functionalized silicon nanoparticles (SiNP) were examined using high-resolution transmission electron microscopy (HRTEM), dynamic light scattering (DLS) and X-ray diffraction (XRD). The amorphous oxide shell of the SiNP was removed by hydrofluoric acid (HF) etching. The resulting hydride (H)-terminated SiNP surfaces were functionalized with styrene via hydrosilylation of phenyl acetylene. Evidences for the styrenyl termination of the SiNP through Si{single bond}C bonds were obtained from diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS), solid-state C nuclear magnetic resonance (NMR) and HRTEM. © 2007 Elsevier B.V. All rights reserved.

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How to cite

APA:

Reindl, A., Cimpean, C.R., Bauer, W., Peukert, W., Kryschi, C., Comanici, R., & Ebbers, A. (2007). Dispersing silicon nanoparticles with a stirred media mill and subsequent functionalization with phenyl acetylene. Colloids and Surfaces A-Physicochemical and Engineering Aspects, 301, 382-387. https://doi.org/10.1016/j.colsurfa.2006.12.073

MLA:

Reindl, Armin, et al. "Dispersing silicon nanoparticles with a stirred media mill and subsequent functionalization with phenyl acetylene." Colloids and Surfaces A-Physicochemical and Engineering Aspects 301 (2007): 382-387.

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