Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties

Journal article
(Original article)


Publication Details

Author(s): Machoke A, Knoke IY, Lopez-Orozco S, Schmiele M, Selvam T, Marthala VRR, Spiecker E, Unruh T, Hartmann M, Schwieger W, Hartmann M, Spiecker E
Journal: Microporous and Mesoporous Materials
Publisher: Elsevier
Publication year: 2014
Volume: 190
Pages range: 324-333
ISSN: 1387-1811


Abstract


The formation of multilamellar MFI-type zeolite has been studied systematically by investigating the crystallization kinetics and the influence of different synthesis parameters under static conditions. Depending on the template amount and alkalinity, multilamellar MFI-type zeolites with different degrees of purity were obtained. In accordance with X-ray diffraction, SAXS and SEM results, highly crystalline multilamellar MFI-type zeolites were obtained within 4 days of crystallization time. Depending on the Si/Al ratio of the synthesis gel, different crystallization rates, textural properties and product morphologies were observed. (C) 2014 Elsevier Inc. All rights reserved.



FAU Authors / FAU Editors

Hartmann, Martin Prof. Dr.
Professur für Katalyse
Machoke, Albert
Lehrstuhl für Chemische Reaktionstechnik
Schmiele, Martin
Lehrstuhl für Kristallographie und Strukturphysik
Schwieger, Wilhelm Prof. Dr.
Professur für Technische Chemie (Reaktionstechnik)
Spiecker, Erdmann Prof. Dr.
Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung)
Unruh, Tobias Prof. Dr.
Professur für Nanomaterialcharakterisierung (Streumethoden)


Additional Organisation
Exzellenz-Cluster Engineering of Advanced Materials
Interdisziplinäres Zentrum, Center for Nanoanalysis and Electron Microscopy (CENEM)


Research Fields

D Catalytic Materials
Exzellenz-Cluster Engineering of Advanced Materials
A2 Nanoanalysis and Microscopy
Exzellenz-Cluster Engineering of Advanced Materials


How to cite

APA:
Machoke, A., Knoke, I.Y., Lopez-Orozco, S., Schmiele, M., Selvam, T., Marthala, V.R.R.,... Spiecker, E. (2014). Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties. Microporous and Mesoporous Materials, 190, 324-333. https://dx.doi.org/10.1016/j.micromeso.2014.02.026

MLA:
Machoke, Albert, et al. "Synthesis of multilamellar MFI-type zeolites under static conditions: The role of gel composition on their properties." Microporous and Mesoporous Materials 190 (2014): 324-333.

BibTeX: 

Last updated on 2019-29-05 at 15:47