The stopped-drop method: A novel setup for containment-free and time-resolved measurements
Magerl A, Schiener A, Seifert S (2016)
Publication Language: English
Publication Status: Published
Publication Type: Journal article, Original article
Publication year: 2016
Journal
Publisher: International Union of Crystallography
Book Volume: 23
Pages Range: 545-550
Journal Issue: 2
DOI: 10.1107/S1600577515023826
Abstract
A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the volution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.
Authors with CRIS profile
Andreas Magerl
Lehrstuhl für Kristallographie und Strukturphysik
Andreas Schiener
Lehrstuhl für Kristallographie und Strukturphysik
Additional Organisation(s)
Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden
Interdisziplinäres Zentrum, Center for Nanoanalysis and Electron Microscopy (CENEM)
Involved external institutions
United States (USA) (US)How to cite
APA:
Magerl, A., Schiener, A., & Seifert, S. (2016). The stopped-drop method: A novel setup for containment-free and time-resolved measurements. Journal of Synchrotron Radiation, 23(2), 545-550. https://dx.doi.org/10.1107/S1600577515023826
MLA:
Magerl, Andreas, Andreas Schiener, and Soenke Seifert. "The stopped-drop method: A novel setup for containment-free and time-resolved measurements." Journal of Synchrotron Radiation 23.2 (2016): 545-550.
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