The stopped-drop method: A novel setup for containment-free and time-resolved measurements

Journal article
(Original article)


Publication Details

Author(s): Magerl A, Schiener A, Seifert S
Journal: Journal of Synchrotron Radiation
Publisher: International Union of Crystallography
Publication year: 2016
Volume: 23
Journal issue: 2
Pages range: 545-550
ISSN: 1600-5775
Language: English


Abstract


A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the volution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.



FAU Authors / FAU Editors

Magerl, Andreas Prof. Dr.
Lehrstuhl für Kristallographie und Strukturphysik
Schiener, Andreas
Lehrstuhl für Kristallographie und Strukturphysik


Additional Organisation
Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden


How to cite

APA:
Magerl, A., Schiener, A., & Seifert, S. (2016). The stopped-drop method: A novel setup for containment-free and time-resolved measurements. Journal of Synchrotron Radiation, 23(2), 545-550. https://dx.doi.org/10.1107/S1600577515023826

MLA:
Magerl, Andreas, Andreas Schiener, and Soenke Seifert. "The stopped-drop method: A novel setup for containment-free and time-resolved measurements." Journal of Synchrotron Radiation 23.2 (2016): 545-550.

BibTeX: 

Last updated on 2018-15-06 at 12:23