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@article{faucris.111494284,
abstract = {The influence of Mg doping in Ca 3(PO 4) 2 on the transformation temperature of β-tricalcium phosphate (β-TCP) to α-tricalcium phosphate (α-TCP) was examined. A maximum substitution by 14 mol% of Mg 2+ on Ca 2+ sites in the β-TCP structure was determined for powders calcinated at 1025±10°C. X-ray powder diffraction analysis (XRPD) in combination with Rietveld method (TOPAS 2.1) was employed for quantitative phase analysis and structural refinement. The synthesized and characterized Mg-doped samples were sintered in air atmosphere in a vertical tube furnace at suitable temperatures ranging from 1460 to 1680°C and subsequently quenched to room temperature, in order to stabilize α-TCP. The β to α transformation temperatures were determined by differential temperature analysis and XRPD analysis. © 2004 Elsevier Ltd. All rights reserved.},
author = {Enderle, Ralph and Götz-Neunhoeffer, Friedlinde and Göbbels, Matthias and Müller, Frank and Greil, Peter},
doi = {10.1016/j.biomaterials.2004.09.017},
faupublication = {yes},
journal = {Biomaterials},
keywords = {α-TCP; β-TCP; Mg substitution; Rietveld refinement; Transformation temperature; Phase transformation temperature; Rietveld method; Room temperature; Structural refinement},
note = {UnivIS-Import:2015-03-09:Pub.2005.nat.dgeo.IGM.LM.influe},
pages = {3379-3384},
peerreviewed = {unknown},
title = {{Influence} of magnesium doping on the phase transformation temperature of {Beta}-{TCP} ceramics examined by {Rietveld} refinement},
volume = {Vol. 26},
year = {2005}
}